%0 Generic %A Othman, Ali %A Eliseeva, Ludmila G. %A M Duksi, Fatima %A G, Polina %A Shalankina, Alyona %D 2021 %T Dataset on the content of vitamin D3 and 25-hydroxyvitamin D3 in 40 pork (Breitov breed) commodities %U https://data.4tu.nl/articles/dataset/Dataset_on_the_content_of_vitamin_D3_and_25-hydroxyvitamin_D3_in_40_pork_Breitov_breed_commodities/17269247/1 %R 10.4121/17269247.v1 %K Vitamin D3 %K 25-hydroxyvitamin D3 %K 25OHD3 %K HPLC %K Pork %K Food analysis %X <p><i>This dataset demonstrates the content of vitamin D</i><i><sub>3</sub></i><i> and 25-hydroxyvitamin D</i><i><sub>3</sub></i><i> (25OHD</i><i><sub>3</sub></i><i>) in boiled, grilled, and raw pork for both lean and whole cuts</i><i> including ribs, tenderloin, shoulder, neck, belly, and center chops</i><i>. </i><i>Total fat content in raw pork cuts is determined by the gravimetric method.</i><i></i></p> <p><i>Quantification analysis using reverse phase </i><i>high performance</i><i> liquid chromatography with UV-DAD</i><i> connected</i><i>.</i><i> </i><i>Purification of fatty acids from proteins was performed using a c18 cartridge, resolving vitamin D</i><i><sub>3</sub></i><i> from its metabolites by subjecting purified samples to polar silica cartridge, purification from sugars by a series of two amino columns. Quantification of </i><i>vitamin D<sub>3</sub> and </i><i>25-hydroxyvitamin D</i><i><sub>3</sub></i><i> by injecting purified extracts on C18 SPE column.</i><i> </i><i>Grilling samples was conducted in an electric combi oven.</i><i></i></p> %I 4TU.ResearchData